3x11 Specialists and Slaves
First Aired: May. 31, 1970 on ABC
Summary: An old enemy of Spidey's, a radiation specialist who once lifted Manhattan into the sky, has been released from jail and promptly revisits Manhattan's nuclear power plant, stuns the outdoor guards with his ray gun, and again commandeers the reactor.
Radiation Specialist: In a little while, you'll no longer be Spider- Man. You will be my slave. Already, the radiation is weakening your will to resist. Soon, your brain will turn to jelly. Your mind will go. You will be a vegetable. A robot with no desire, but to serve me!